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dc.contributor.authorDeev, S. L.en
dc.contributor.authorKhalymbadzha, I. A.en
dc.contributor.authorShestakova, T. S.en
dc.contributor.authorCharushin, V. N.en
dc.contributor.authorChupakhin, O. N.en
dc.date.accessioned2020-09-29T09:45:37Z-
dc.date.available2020-09-29T09:45:37Z-
dc.date.issued2019-
dc.identifier.citation15N labeling and analysis of 13C-15N and 1H-15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles / S. L. Deev, I. A. Khalymbadzha, T. S. Shestakova, V. N. Charushin, et al. . — DOI 10.1039/c9ra04825a // RSC Advances. — 2019. — Vol. 46. — Iss. 9. — P. 26856-26879.en
dc.identifier.issn2046-2069-
dc.identifier.otherhttps://pubs.rsc.org/en/content/articlepdf/2019/ra/c9ra04825apdf
dc.identifier.other1good_DOI
dc.identifier.other27a92a3a-ae20-42e5-b68e-1b4168b5403dpure_uuid
dc.identifier.otherhttp://www.scopus.com/inward/record.url?partnerID=8YFLogxK&scp=85071649721m
dc.identifier.urihttp://elar.urfu.ru/handle/10995/90010-
dc.description.abstractThis review provides a generalization of effective examples of 15N labeling followed by an analysis of 13C-15N (JCN) and 1H-15N (JHN) coupling constants in solution as a tool to study the structural aspects and pathways of chemical transformations (e.g., rearrangements and ring-chain tautomerisms) in monocyclic and fused nitrogen heterocycles. This approach allows us to significantly expand and supplement the scope of NMR techniques for heterocyclic compounds. Moreover, methods for the incorporation of 15N atoms into the cores of various N-heterocycles have been collected in this work. This journal is © The Royal Society of Chemistry.en
dc.description.sponsorshipRussian Foundation for Basic Research, RFBR: 17-03-01029en
dc.description.sponsorshipMinistry of Science and Higher Education of the Russian Federation: 4.6351.2017/8.9en
dc.description.sponsorshipThis work was supported by the Ministry of Science and Higher Education of the Russian Federation (State contract 4.6351.2017/8.9) and the Russian Foundation for Basic Research (grant 17-03-01029).en
dc.format.mimetypeapplication/pdfen
dc.language.isoenen
dc.publisherRoyal Society of Chemistryen
dc.rightsinfo:eu-repo/semantics/openAccessen
dc.rightscc-byother
dc.sourceRSC Advancesen
dc.subjectCHEMICAL REACTIONSen
dc.subjectNITROGENen
dc.subjectCHEMICAL TRANSFORMATIONSen
dc.subjectCOUPLING CONSTANTSen
dc.subjectHETEROCYCLIC COMPOUNDen
dc.subjectN-HETEROCYCLESen
dc.subjectNITROGEN HETEROCYCLESen
dc.subjectNMR TECHNIQUESen
dc.subjectRING-CHAIN TAUTOMERISMen
dc.subjectSTRUCTURAL ASPECTSen
dc.subjectCHEMICAL ANALYSISen
dc.title15N labeling and analysis of 13C-15N and 1H-15N couplings in studies of the structures and chemical transformations of nitrogen heterocyclesen
dc.typeReviewen
dc.typeinfo:eu-repo/semantics/reviewen
dc.typeinfo:eu-repo/semantics/publishedVersionen
dc.identifier.doi10.1039/c9ra04825a-
dc.identifier.scopus85071649721-
local.affiliationUral Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federationen
local.affiliationI. Ya. Postovsky Institute of Organic Synthesis, 22 S. Kovalevskoy Street, Yekaterinburg, 620219, Russian Federationen
local.contributor.employeeDeev, S.L., Ural Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federation, I. Ya. Postovsky Institute of Organic Synthesis, 22 S. Kovalevskoy Street, Yekaterinburg, 620219, Russian Federationru
local.contributor.employeeKhalymbadzha, I.A., Ural Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federationru
local.contributor.employeeShestakova, T.S., Ural Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federationru
local.contributor.employeeCharushin, V.N., Ural Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federation, I. Ya. Postovsky Institute of Organic Synthesis, 22 S. Kovalevskoy Street, Yekaterinburg, 620219, Russian Federationru
local.contributor.employeeChupakhin, O.N., Ural Federal University, 19 Mira Street, Yekaterinburg, 620002, Russian Federation, I. Ya. Postovsky Institute of Organic Synthesis, 22 S. Kovalevskoy Street, Yekaterinburg, 620219, Russian Federationru
local.description.firstpage26856-
local.description.lastpage26879-
local.issue9-
local.volume46-
dc.identifier.wos000483739800041-
local.identifier.pure10769588-
local.identifier.eid2-s2.0-85071649721-
local.fund.rffi17-03-01029-
local.identifier.wosWOS:000483739800041-
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