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dc.contributor.authorRakhmatullin, A.en
dc.contributor.authorBrusko, V. V.en
dc.contributor.authorShcherbitskaya, E. R.en
dc.contributor.authorPolovov, I. B.en
dc.contributor.authorBakirov, R.en
dc.contributor.authorBessada, C.en
dc.date.accessioned2022-10-19T05:25:11Z-
dc.date.available2022-10-19T05:25:11Z-
dc.date.issued2022-
dc.identifier.citationSolid-state 31P and 109Ag CP/MAS NMR as a powerful tool for studying of silver(I) complexes with N-thiophosphorylated thiourea and thioamide ligands / A. Rakhmatullin, V. V. Brusko, E. R. Shcherbitskaya et al. // Magnetic Resonance in Chemistry. — 2022. — Vol. 60. — Iss. 9. — P. 893-900.en
dc.identifier.issn7491581-
dc.identifier.otherhttps://www.scopus.com/inward/record.uri?eid=2-s2.0-85132868690&doi=10.1002%2fmrc.5294&partnerID=40&md5=cf6cc0aca0130f79c3246087b8dcfcb5link
dc.identifier.urihttp://elar.urfu.ru/handle/10995/118336-
dc.description.abstractA family of three- and four-coordinated silver(I) complexes of formulas [Ag(PPh3)2L], [Ag(PPh3)L], and [AgL]n with N-thiophosphorylated thiourea and thioamide ligands of general formula RC(S)NHP(S)(OPri)2 [R = Ph, PhNH, iPrNH, tBuNH, NH2] have been studied by solid-state 109Ag and 31P CPMAS NMR spectroscopy. 109Ag NMR spectra have provided valuable structural information about Ag coordination, which is in good accordance with the available crystal structure data. The data presented in this work represent a significant addition to the available 109Ag chemical shifts and chemical shifts anisotropies. The silver chemical shift ranges for different P,S-environments and coordination state were discussed in detail. The 1J(31P–107/109Ag) and 2J(31P–31P) values were determined and analyzed. © 2022 John Wiley & Sons Ltd.en
dc.description.sponsorshipKazan Federal University: Priority-2030en
dc.description.sponsorshipFinancial support from the IR-RMN-THC Fr3050 CNRS for conducting the research is gratefully acknowledged. This paper has been supported by the Kazan Federal University Strategic Academic Leadership Program (Priority-2030).en
dc.description.sponsorshipFinancial support from the IR-RMN-THC Fr3050 CNRS for conducting the research is gratefully acknowledged. This paper has been supported by the Kazan Federal University Strategic Academic Leadership Program (Priority-2030).en
dc.format.mimetypeapplication/pdfen
dc.language.isoenen
dc.publisherJohn Wiley and Sons Ltden
dc.rightsinfo:eu-repo/semantics/openAccessen
dc.sourceMagnetic Resonance in Chemistryen
dc.subject31P AND 109AG NMRen
dc.subjectN-THIOPHOSPHORYLTHIOUREAen
dc.subjectPOLYNUCLEAR COMPLEXESen
dc.subjectSILVER(I) COMPLEXESen
dc.subjectSOLID-STATE NMRen
dc.subjectLIGANDen
dc.subjectSILVERen
dc.subjectTHIOAMIDEen
dc.subjectTHIOUREAen
dc.subjectCHEMISTRYen
dc.subjectNUCLEAR MAGNETIC RESONANCE SPECTROSCOPYen
dc.subjectPROCEDURESen
dc.subjectLIGANDSen
dc.subjectMAGNETIC RESONANCE SPECTROSCOPYen
dc.subjectSILVERen
dc.subjectTHIOAMIDESen
dc.subjectTHIOUREAen
dc.titleSolid-state 31P and 109Ag CP/MAS NMR as a powerful tool for studying of silver(I) complexes with N-thiophosphorylated thiourea and thioamide ligandsen
dc.typeArticleen
dc.typeinfo:eu-repo/semantics/articleen
dc.typeinfo:eu-repo/semantics/publishedVersionen
dc.identifier.doi10.1002/mrc.5294-
dc.identifier.scopus85132868690-
local.contributor.employeeRakhmatullin, A., Conditions Extrêmes et Materiaux: Haute Température et Irradiation, CEMHTI, UPR 3079-CNRS Univ Orleans, Orléans, Franceen
local.contributor.employeeBrusko, V.V., A. M. Butlerov Chemistry Institute, Kazan State University, Kazan, Russian Federationen
local.contributor.employeeShcherbitskaya, E.R., JSC “NIIneftepromchim”, Kazan, Russian Federationen
local.contributor.employeePolovov, I.B., Department of Rare Metals and Nanomaterials, Institute of Physics and Technology, Ural Federal University, Ekaterinburg, Russian Federationen
local.contributor.employeeBakirov, R., Department of Technology of Mechanical Engineering and Instrument Making, Votkinsk Branch of Kalashnikov Izhevsk State Technical University, Votkinsk, Russian Federationen
local.contributor.employeeBessada, C., Conditions Extrêmes et Materiaux: Haute Température et Irradiation, CEMHTI, UPR 3079-CNRS Univ Orleans, Orléans, Franceen
local.description.firstpage893-
local.description.lastpage900-
local.issue9-
local.volume60-
dc.identifier.wos000816987800001-
local.contributor.departmentConditions Extrêmes et Materiaux: Haute Température et Irradiation, CEMHTI, UPR 3079-CNRS Univ Orleans, Orléans, Franceen
local.contributor.departmentA. M. Butlerov Chemistry Institute, Kazan State University, Kazan, Russian Federationen
local.contributor.departmentJSC “NIIneftepromchim”, Kazan, Russian Federationen
local.contributor.departmentDepartment of Rare Metals and Nanomaterials, Institute of Physics and Technology, Ural Federal University, Ekaterinburg, Russian Federationen
local.contributor.departmentDepartment of Technology of Mechanical Engineering and Instrument Making, Votkinsk Branch of Kalashnikov Izhevsk State Technical University, Votkinsk, Russian Federationen
local.identifier.pure30701945-
local.identifier.eid2-s2.0-85132868690-
local.identifier.wosWOS:000816987800001-
local.identifier.pmid35712821-
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