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http://elar.urfu.ru/handle/10995/116227
Полная запись метаданных
Поле DC | Значение | Язык |
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dc.contributor.author | Tolkacheva, A. S. | en |
dc.contributor.author | Shkerin, S. N. | en |
dc.contributor.author | Petrova, S. A. | en |
dc.contributor.author | Fedorova, O. M. | en |
dc.contributor.author | Titova, S. G. | en |
dc.contributor.author | Leonidov, I. I. | en |
dc.date.accessioned | 2022-07-18T12:59:03Z | - |
dc.date.available | 2022-07-18T12:59:03Z | - |
dc.date.issued | 2022-07 | - |
dc.identifier.citation | In Situ Synthesis, Structural Chemistry and Vibrational Spectroscopy of Zn-doped Ca5Mg4(VO4)6 / A. S. Tolkacheva, S. N. Shkerin, S. A. Petrova, O. M. Fedorova, S. G. Titova, I. I. Leonidov // Chimica Techno Acta. — 2022. — Vol. 9, No. 2. — № 20229201. | en |
dc.identifier.issn | 2411-1414 | online |
dc.identifier.uri | http://elar.urfu.ru/handle/10995/116227 | - |
dc.description | We are grateful to Dr. Olga G. Reznitskikh (ISSC UB RAS), Dr. Elena A. Sherstobitova (IMP UB RAS) and Dr. Nikolai I. Moskalenko (IHTE UB RAS) for technical assistance. The crystallographic and spectroscopic studies were carried out in the Shared Access Centers at IMET UB RAS and IHTE UB RAS, respectively. | en |
dc.description | Received: 18.08.2021. Revised: 17.03.2022. Accepted: 17.03.2022. Available online: 23.03.2022. | en |
dc.description.abstract | The phase formation of the solid solution Ca5Mg4–xZnx(VO4)6 (0≤x≤4) was studied in situ using differential scanning calorimetry and hightemperature X-Ray powder diffraction (XRPD). XRPD analysis shows the appearance of unavoidable secondary pyrovanadate phases using conventional synthesis methods. The local structure of the solid solution was verified by vibrational spectroscopy. The analysis of the infrared and Raman spectroscopy data allows establishing the main features between vanadate garnets and their isostructural analogs among natural silicates. | en |
dc.description.sponsorship | This study was funded by the Research Programs No. AAAA-A19-119020190042-7 and No. АААА-А19-119020190044-1 (IHTE UB RAS). | en |
dc.format.mimetype | application/pdf | en |
dc.language.iso | en | en |
dc.publisher | Уральский федеральный университет | ru |
dc.relation.ispartof | Chimica Techno Acta. 2022. Vol. 9. № 2 | en |
dc.relation.haspart | Ural Federal University | en |
dc.subject | CRYSTAL STRUCTURE | en |
dc.subject | VIBRATIONAL SPECTROSCOPY | en |
dc.subject | X-RAY DIFFRACTION | en |
dc.subject | CERAMICS | en |
dc.subject | DIFFERENTIAL SCANNING CALORIMETRY | en |
dc.subject | PYROVANADATE | en |
dc.subject | GARNET | en |
dc.title | In Situ Synthesis, Structural Chemistry and Vibrational Spectroscopy of Zn-doped Ca5Mg4(VO4)6 | en |
dc.type | Article | en |
dc.type | info:eu-repo/semantics/article | en |
dc.type | info:eu-repo/semantics/publishedVersion | en |
dc.identifier.rsi | https://www.elibrary.ru/item.asp?id=49170458 | - |
dc.identifier.doi | 10.15826/chimtech.2022.9.2.01 | - |
local.issue | 2 | - |
local.volume | 9 | - |
local.contributor | Tolkacheva, Anna S. | en |
local.contributor | Shkerin, Sergey N. | en |
local.contributor | Petrova, Sofya A. | en |
local.contributor | Fedorova, Olga M. | en |
local.contributor | Titova, Svetlana G. | en |
local.contributor | Leonidov, Ivan I. | en |
Располагается в коллекциях: | Chimica Techno Acta |
Файлы этого ресурса:
Файл | Описание | Размер | Формат | |
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cta-2022-2-01.pdf | 1,07 MB | Adobe PDF | Просмотреть/Открыть |
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