Please use this identifier to cite or link to this item: http://hdl.handle.net/10995/112217
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dc.contributor.authorValeeva, A. A.en
dc.contributor.authorRempel, A. A.en
dc.contributor.authorPfitzner, A.en
dc.date.accessioned2022-05-12T08:30:44Z-
dc.date.available2022-05-12T08:30:44Z-
dc.date.issued2015-
dc.identifier.citationValeeva A. A. Elimination of Vacancies in Titanium Monoxide under High Pressure in Combination with High Temperature / A. A. Valeeva, A. A. Rempel, A. Pfitzner // Monatshefte fur Chemie. — 2015. — Vol. 146. — Iss. 8. — P. 1205-1209.en
dc.identifier.issn0026-9247-
dc.identifier.otherAll Open Access, Green3
dc.identifier.urihttp://hdl.handle.net/10995/112217-
dc.description.abstractThe material design with controlled structure was performed on titanium monoxide with structural vacancies on both sublattices. The polycrystalline powder of disordered titanium monoxide TiO0.98 with B1 structure was subjected to high pressures up to 60 kbar and high temperatures up to 2273 K. The X-ray powder diffraction of as-prepared and treated powders revealed cubic single-phase crystals. The lattice constant of this phase increased from 417.6(3) to 418.5(3) pm due to decreasing vacancy concentration on the titanium sublattice from 13.3 to 8.5 at.% after a highest pressure-highest temperature treatment for 1 h. Graphical abstract: [Figure not available: see fulltext.] © 2015 Springer-Verlag Wien.en
dc.description.sponsorshipWe are grateful to Dr. M. Andratschke, F. Rau, and U. Schiessl for their help during the experiments. This work was financially supported by the AvH Foundation, RFBR Nos. 14-03-00869 and 15-03-00453.en
dc.format.mimetypeapplication/pdfen
dc.language.isoenen
dc.publisherSpringer-Verlag Wienen1
dc.publisherSpringer Science and Business Media LLCen
dc.rightsinfo:eu-repo/semantics/openAccessen
dc.sourceMonatsh. Chem.2
dc.sourceMonatshefte fur Chemieen
dc.subjectNON-STOICHIOMETRYen
dc.subjectSTRUCTURAL VACANCYen
dc.subjectVACANCY ELIMINATIONen
dc.subjectXRDen
dc.titleElimination of Vacancies in Titanium Monoxide under High Pressure in Combination with High Temperatureen
dc.typeArticleen
dc.typeinfo:eu-repo/semantics/articleen
dc.typeinfo:eu-repo/semantics/submittedVersionen
dc.identifier.scopus84927534488-
local.contributor.employeeValeeva, A.A., Institute of Solid State Chemistry, Ural Branch of the Russian Academy of Sciences, Pervomaiskaya 91, Ekaterinburg, 620990, Russian Federation, Ural Federal University Named after the First President of Russia B.N. Yeltsin, Mira 19, Ekaterinburg, 620002, Russian Federation; Rempel, A.A., Institute of Solid State Chemistry, Ural Branch of the Russian Academy of Sciences, Pervomaiskaya 91, Ekaterinburg, 620990, Russian Federation, Ural Federal University Named after the First President of Russia B.N. Yeltsin, Mira 19, Ekaterinburg, 620002, Russian Federation; Pfitzner, A., Institute of Inorganic Chemistry, Regensburg University, Universitätsstr. 31, Regensburg, 93040, Germanyen
local.description.firstpage1205-
local.description.lastpage1209-
local.issue8-
local.volume146-
local.contributor.departmentInstitute of Solid State Chemistry, Ural Branch of the Russian Academy of Sciences, Pervomaiskaya 91, Ekaterinburg, 620990, Russian Federation; Ural Federal University Named after the First President of Russia B.N. Yeltsin, Mira 19, Ekaterinburg, 620002, Russian Federation; Institute of Inorganic Chemistry, Regensburg University, Universitätsstr. 31, Regensburg, 93040, Germanyen
local.identifier.pure431163-
local.identifier.eid2-s2.0-84927534488-
local.fund.rffi14-03-00869
local.fund.rffi15-03-00453
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