Reaction of sodium 4-acetyl-1-phenyl-1 H -1,2,3-triazol-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide

Abstract

The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure of synthesized compound was characterized by spectroscopic methods such as 1H NMR, 13C NMR, IR, mass spectrometry and X-ray diffraction. © 2019 Author(s).